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1 article(s) from Cludius-Brandt, Stephan

[3 + 2]-Cycloadditions of nitrile ylides after photoactivation of vinyl azides under flow conditions

Stephan Cludius-Brandt,
Lukas Kupracz and
Andreas Kirschning

Beilstein J. Org. Chem. 2013, 9, 1745–1750, doi:10.3762/bjoc.9.201

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Scheme 1: Formation of azirines 2 from vinyl azides 1, photoinduced ring-opening to the nitrile ylides 3, and...

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Scheme 2: Solid-phase assisted synthesis of vinyl azides 1 from alkenes 6 under flow conditions [9].

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Scheme 3: Schematic presentation of the flow set-up for the synthesis of 2H-azirines 2 under inductive heatin...

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Scheme 4: Photoinduced cycloadditions of vinyl azides 1a–f and electron-deficient alkenes 4a–d. All experimen...

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Scheme 5: Photoinduced cycloaddtion of vinyl azide 1c and diisopropyl azodicarboxylate (4e). The experiment w...

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Scheme 6: Photoinduced cycloaddtion of vinyl azide 1b and alkyne 4f. The experiment was conducted at room tem...

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Scheme 7: Formation of 2,5-dihydrooxazole 9 starting from vinyl azide 1g under flow conditions (c = 0.01 M, f...

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Published 26 Aug 2013

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